| Edition |
2nd ed. |
| Description |
1 online resource (xvi, 574 pages) : illustrations |
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text txt rdacontent |
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computer c rdamedia |
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online resource cr rdacarrier |
| Summary |
This book contains 60 quality 2D NMR data sets following an introductory section describing the methodology employed. Many other books describe the methods used, but none offer a large number of problems. Instructors at universities and colleges at the present time are forced to cobble together problems from a wide range of sources. The fragmentary approach to assembling course materials has a negative impact on course continuity and thus adversely impacts student retention. This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty. . Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra . Contains 20 known and 20 unknown structure determination problems . Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing. |
| Contents |
PART I: Background and Methods Chapter 1: Introduction Chapter 2: Instrumental Considerations Chapter 3: Data Collection, Processing, and Plotting Chapter 4: 1H and 13C Chemical Shifts Chapter 5: Symmetry and Topicity Chapter 6: Through-Bond Effects: Spin-Spin (J) Coupling Chapter 7: Through-Space Effects: the Nuclear Overhauser Effect (NOE) Chapter 8: Molecular Dynamics Chapter 9: Strategies for Assigning Molecules Chapter 10: Strategies for Elucidating Unknown Molecular Structures PART II: Problems Chapter 11 Simple Assignment Problems Chapter 12: Complex Assignment Problems Chapter 13: Simple Unknown Problems Chapter 14: Complex Unknown Problems Chapter 15: NMR Resonance Assignment Problems Chapter 16: NMR Unknown Problems. |
| Summary |
"The second edition of this book comes with a number of new figures, passages, and problems. Increasing the number of figures from 290 to 448 has necessarily added considerable length, weight, and, expense. It is my hope that the book has not lost any of its readability and accessibility. I firmly believe that most of the concepts needed to learn organic structure determination using nuclear magnetic resonance spectroscopy do not require an extensive mathematical background. It is my hope that the manner in which the material contained in this book is presented both reflects and validates this belief"-- Provided by publisher |
| Bibliography |
Includes bibliographical references and index. |
| Note |
Machine generated contents note: PART I: Background and Methods Chapter 1: Introduction Chapter 2: Instrumental Considerations Chapter 3: Data Collection, Processing, and Plotting Chapter 4: 1H and 13C Chemical Shifts Chapter 5: Symmetry and Topicity Chapter 6: Through-Bond Effects: Spin-Spin (J) Coupling Chapter 7: Through-Space Effects: the Nuclear Overhauser Effect (NOE) Chapter 8: Molecular Dynamics Chapter 9: Strategies for Assigning Molecules Chapter 10: Strategies for Elucidating Unknown Molecular Structures PART II: Problems Chapter 11 Simple Assignment Problems Chapter 12: Complex Assignment Problems Chapter 13: Simple Unknown Problems Chapter 14: Complex Unknown Problems. |
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Print version record. |
| Subject |
Molecular structure.
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Organic compounds -- Analysis.
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Nuclear magnetic resonance spectroscopy.
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Structure moléculaire.
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Composés organiques -- Analyse.
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Spectroscopie de la résonance magnétique nucléaire.
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molecular structure.
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Molecular structure
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Nuclear magnetic resonance spectroscopy
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Organic compounds -- Analysis
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| Other Form: |
Print version: Simpson, Jeffrey H. Organic structure determination using 2-D NMR spectroscopy. 2nd ed. San Diego, CA : Academic Press, 2012 9780123849700 (DLC) 2011038670 (OCoLC)755640744 |
| ISBN |
9780123849700 (electronic bk.) |
|
0123849705 (electronic bk.) |
| Standard No. |
AU@ 000049014134 |
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CHBIS 009942906 |
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CHVBK 303939923 |
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DEBBG BV042305185 |
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DEBSZ 367764288 |
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NZ1 15189088 |
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NZ1 15622201 |
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