| Description |
1 online resource : illustrations |
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text txt rdacontent |
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computer c rdamedia |
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online resource cr rdacarrier |
| Series |
Annual reports on NMR spectroscopy, 0066-4103 ; volume 84 |
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Annual reports on NMR spectroscopy ; v. 84.
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| Bibliography |
Includes bibliographical references and index. |
| Note |
Online resource; title from PDF title page (ScienceDirect, viewed March 9, 2015). |
| Summary |
Annual Reports on NMR Spectroscopy provides a thorough and in-depth accounting of progress in nuclear magnetic resonance (NMR) spectroscopy and its many applications. Nuclear magnetic resonance (NMR) is an analytical tool used by chemists and physicists to study the structure and dynamics of molecules. In recent years, no other technique has gained as much significance as NMR spectroscopy. It is used in all branches of science in which precise structural determination is required and in which the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a premier means for the specialist and non-specialist alike to become familiar with new techniques and applications of NMR spectroscopy. |
| Contents |
Front Cover; Annual Reports on NMR Spectroscopy; Copyright; Contents; Contributors; Preface; Chapter 1: Applications of 1H-15N Long-Range Heteronuclear Shift Correlation and 15N NMR in Alkaloid Chemistry; 1. Introduction; 2. Previous Reviews; 3. Experiments and Parametric Considerations; 3.1. 15N Chemical Shift Referencing; 3.2. Pulse Width and Gradient Considerations; 3.3. 15N Chemical Shift Calculation and Prediction; 3.3.1. Validating 15N Chemical Shift Prediction; 3.3.2. Setting F1 Spectral Windows; 3.3.3. Structure Verification Using a 15N Content Data Base |
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3.3.4. Enhancing 15N Chemical Shift Prediction with a ``User Trained Database4. Computer-Assisted Structure Elucidation-The Impact of 15N Data; 5. Covariance Calculation of 13C-15N Heteronuclear Shift Correlation Spectra; 6. Applications of Long-Range 1H-15N Heteronuclear Shift Correlation to Alkaloids not Previously Reviewed; 6.1. Stylissadines A and B-Tetrameric Pyrrole-Imidazole Alkaloids; 7. Applications of Long-Range 1H-15N Heteronuclear Shift Correlation to Alkaloids; 7.1. Five- and Six-Membered Ring Alkaloids |
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7.1.1. Characterization of Pyrrole Sulfoxides from Allium Subgenus melanocrommyum7.1.2. Nagelamide T Isolated from Pacific Sponges; 7.1.3. Characterization of Benzosceptrin C-A Bromopyrrole Alkaloid from the Sponge Agelas sp.; 7.1.4. An Unusual 1-Phenyl-4-Pyridone Alkaloid from Aspergillus niger; 7.1.5. Farinomalein-A Maleimide-Bearing Alkaloid from the Entomopathogenic Fungus Paecilomyces farinosus; 7.1.6. Synthesis of 7-15N-Oroidin; 7.1.7. Structural Characterization of Donnazoles A and B, Novel Pyrrole-Aminoimidazole Alkaloids from the Marine Sponge A ... |
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7.1.8. Characterization of New Cytotoxic Thiadiazole Alkaloids from the Ascidian Polycarpa aurata7.2. Tropane Alkaloids; 7.3. Indoles, Oxindoles, and Related Alkaloids; 7.3.1. Total Synthesis of Flustramine C; 7.3.2. 15N CP-MAS NMR of Stereoisomeric Oxindole Alkaloids from Cat s Claw (Uncaria tomentosa); 7.3.3. Secondary Prenylated Indole Alkaloids from a Marine-Derived Fungus Aspergillus carneus; 7.3.4. Aplicyanins-Cytotoxic Bromindole Alkaloids; 7.4. Strychnos Alkaloids; 7.5. Azindoles; 7.6. Vinca Alkaloids; 7.6.1. 15N Measurements for Vinblastine and Vincristine |
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7.7. Other Indole Alkaloids7.7.1. Structure and Solvent Effects on the 13C and 15N Shifts of Indoloquinoline Alkaloids; 7.7.2. Synthesis-Driven Mapping of the Dictyodendrin Alkaloids; 7.7.3. Structural Characterization of Pseudocerosin-An Indolic Azafulvene Alkaloid from the Flatworm Pseudoceros indicus; 7.7.4. Aspergilazine A-A Diketopiperazine Dimer with a Rare N1-C6 Linkage; 7.7.5. Indolo[2,3-b]quinoline Alkaloid Derivatives as Potential Anticancer Drugs; 7.7.6. Mycoleptodiscins-Cytotoxic Alkaloids from an Endophytic Fungus; 7.8. Carboline and Carbazole-Derived Alkaloids |
| Subject |
Nuclear magnetic resonance spectroscopy.
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Magnetic Resonance Spectroscopy |
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Spectroscopie de la résonance magnétique nucléaire.
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SCIENCE -- Chemistry -- Analytic.
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Nuclear magnetic resonance spectroscopy
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| Genre/Form |
Festschriften
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Festschriften.
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| Added Author |
Webb, G. A. (Graham Alan), 1935- editor.
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| Other Form: |
Print version: 9780128021248 |
| ISBN |
9780128023327 (electronic bk.) |
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0128023325 (electronic bk.) |
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9780128021248 |
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0128021241 |
| Standard No. |
AU@ 000055409463 |
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AU@ 000068482343 |
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CHBIS 010550007 |
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CHVBK 341936286 |
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GBVCP 825925924 |
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UKMGB 017050422 |
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